☰ Contents · Chemistry

Laboratory sessions

Lessons 50 · 1 lessons · I.R. Asqarov, K. G‘opirov, N.X. To‘xtaboyev. Chemistry Grade 8, revised 4th edition. “Yangiyul Poligraph Service”, Tashkent, 2019
50

Laboratory sessions (1–10)

Textbook: pp. 200–204
GoalPlan and analyse 10 laboratory sessions on the year’s topics: observation table, conclusion, equations and safety rules.
New words
laboratory work · laboratoriya ishiobservation table · kuzatish jadvaliconclusion · xulosapersonal protective equipment · shaxsiy himoya vositalari
Explanation

Laboratory sessions connect the theory of the year with experiment. The list: 1) preparing zinc hydroxide and its reaction with acid and alkali (amphoteric nature): ZnCl₂ + 2NaOH → Zn(OH)₂↓ + 2NaCl; Zn(OH)₂ + 2HCl → ZnCl₂ + 2H₂O; the precipitate dissolves in excess alkali, while copper(II) hydroxide is not amphoteric; 2) building ball-and-stick models of the crystal lattices of KCl, sulfur and iodine; 3) qualitative reactions of HCl, NaCl, NaBr and NaI with AgNO₃ (white, pale yellow, yellow precipitate) and detecting iodine with starch; 4) detecting chloride ions in a soil solution; 5) halogens displacing one another; 6) dissolving iodine in water and in an organic solvent; 7) getting to know samples of sulfur and its natural compounds; 8) detecting the sulfate ion in various solutions with BaCl₂; 9) preparing ammonia from an ammonium salt and studying its properties; 10) getting to know samples of mineral fertilizers. All work is done under the teacher’s guidance, in goggles, gloves and apron, in small amounts; only the teacher works with chlorine or bromine water, ammonia and acids; nothing is smelled or tasted; if a solution spills, rinse with plenty of water and tell the teacher. Benzene causes cancer, so we do not use it here: the teacher chooses the solvent. Only session 2 (models) can also be done at home with simple materials (plasticine, sticks); the samples in sessions 7 and 10 are looked at only at school, when the teacher shows them.

Worked examples
Lab session 8: BaCl₂ added to H₂SO₄, Na₂SO₄, CuSO₄ and Al₂(SO₄)₃ gives white BaSO₄ in every tube: Ba²⁺ + SO₄²⁻ → BaSO₄↓. Mᵣ(Al₂(SO₄)₃) = 2·27 + 3·96 = 342; 1 mol of the salt gives 3 mol BaSO₄.
Session 7 table: sulfur Mᵣ(S₈) = 256 (or Aᵣ = 32), pyrite FeS₂ = 120, zinc blende ZnS = 97, gypsum CaSO₄·2H₂O = 40 + 32 + 64 + 36 = 172. S, FeS₂ and ZnS are insoluble in water, while gypsum is slightly soluble.
Class activity

“Lab scheme”: choose 3 of the 10 sessions and for each make an A4 sheet: aim, equipment, steps (drawing), expected result, equation, safety rule. Mark which sessions are safe at home (only building models) and which only in the school laboratory.

Practice
1
How do we show the amphoteric nature of Zn(OH)₂? Two equations.
2
In session 3 what are the precipitate colours when AgNO₃ is added to HCl, NaCl, NaBr, NaI?
3
Calculate Mᵣ of gypsum CaSO₄·2H₂O.
4
Why do only teachers work with chlorine and bromine water in the laboratory?